By J. F. Jackson, L. Mandelkern (auth.), Roger S. Porter, Julian F. Johnson (eds.)
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Additional resources for Analytical Calorimetry: Proceedings of the American Chemical Society Symposium on Analytical Calorimetry, San Francisco, California, April 2–5, 1968
2. 3. 4. 5. 6. 7. 8. 9. B. Wunderlich and M. Dole, J. , 24, 201 (1957). A. , and L. , 80, 3178 (1958). L. G. Fatou, R. Denison and J. Justin. J. Polymer Sci. B3, 803 (1965). W. A. B. , in press. J. W. D. Mak, J. Polymer Sci. B4, 147 (1966). S. C. H. Elliot, J. , 31, 453, (1958). W. D. Ilavsky, in preparation. J. Cottam, J. Appl. , 2, 1853 (1965). W. A. Scott, J. Appl. , 11, 2325 (1967) . MEASUREMENT OF THE CRYSTALLIZATION RATES OF POLYfiJERS BY DIFFERENTIAL SCANNING CALORH'lETRY J. R. Knox Avisun Corporation Marcus Hook, Pennsylvania Measurements of the crystallization rates of polY1"1ers are of great importance both from a practical and a basic viewpoint.
REFERENCES 1. Fisher, E. W. and Schmidt, G. , Angew. , 74, 551 (1962). 2. Statton, W. O. and Geil, P. , ~ App1. Poly. , 1,357 (1960). 3. Takayanagi, M. , Mem. Fac. Engng. Kyushu, 24, 33 (1965) . 4. Bair, H. , Salovey, R. and Huseby, T. , Polymer, ~, 9 (1967). 5. Blundell, D. , Keller, A. and Kovacs, A. , ~, 481 (1966). 6. Hoffman, J. D. and Lauritzen, J. , 297 (1961). 7. Quinn, F. , Jr. , J. Am. Chern. , Rubber Chern. Tech-:-;-32, 1403Tl959J. 8. Flory, P. J. , ~ Am. Chern. , 85, 3548 (1963). 9· Broadhurst, M.
Therefore, it is necessary to separate the crystals from the mother liquor at the crystallization temperature to inhibit recrystallization during DTA. It is desirable to extend observations to the highest possible temperatures. 1% w solutions of polyethylene in p-xylene produced no crystals even in 1000 minutes at 90°C. so samples representative of higher temperatures were prepared by annealing. A suspension prepared at 70°C. was annealed at 90° for varying lengths of time, and the crystals were separated at the annealing temperature.
Analytical Calorimetry: Proceedings of the American Chemical Society Symposium on Analytical Calorimetry, San Francisco, California, April 2–5, 1968 by J. F. Jackson, L. Mandelkern (auth.), Roger S. Porter, Julian F. Johnson (eds.)